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Residual Solvents by Teledyne Tekmar HT3 Headspace Autosampler and Varian 4000 GCMS

Many solvents are used in the manufacturing of pharmaceutical products, substances, and excipients. In an order to protect the health of the patient, pharmaceutical companies have adopted methods that will r ...

Resource - Susan Gilbert - 19th Dec 2011 - 0 comments

The Use of the Teledyne Tekmar HT3 for Analysing Selected Residual Solvents in Pharmaceutical Products and Ingredients

Many different solvents are used in the manufacture of pharmaceutical products. To protect the health of the patient, the International Conference on Harmonization (ICH) has published guidelines on the classi ...

Resource - admin - 19th Dec 2011 - 0 comments

The Automated Sample Preparation and Analysis of a Pharmaceutical Cream using the Focus Sample Processing Robot

The extraction of active ingredients from pharmaceutical products, especially creams, can often be a long and tedious process involving many steps and using strongly acidic and basic reagents. An automated e ...

Resource - Susan Gilbert - 18th Apr 2011 - 0 comments

Implementation of USP <467> 'Residual Solvents' using a GERSTEL MPS 2 Syringe Based Headspace Autosampler

USP <467> Residual Solvents is a general chapter in the US Pharmacopeia that describes a headspace gas chromatographic method for the determination of residual solvents in pharmaceutical products, active ...

Resource - Susan Gilbert - 21st Dec 2010 - 0 comments

Extraction of Leachables from Rubber Samples using the GERSTEL MPS PrepStation

The analysis of leachables from polymeric components in pharmaceutical systems is essential to ensure the safe delivery of drugs to a patient. A typical extraction technique would be to ultrasonicate the comp ...

Resource - admin - 9th Sep 2010 - 0 comments

Determination of Residual Solvents in Injectable Media by HS-GC-FID

A wide range of solvents can be used in the production of pharmaceutical products. In order to protect the patient, pharmaceutical companies are adopting techniques that both reduce the toxicity of residual ...

Resource - admin - 9th Sep 2010 - 0 comments

Automated, Accurate and Reproducible Fatty Acid Derivatisation

The ability to automate routine laboratory tasks can be beneficial in both saving staff time and improving the reproducibility of the procedure. This note describes the use of the GERSTEL MPS PrepStation for ...

Resource - admin - 9th Sep 2010 - 0 comments